Crystallography Open Database

Information card for entry 4069795

Preview

Coordinates	4069795.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	3c, (dippdmae)Pt(tBuCCPh)
Formula	C22 H38 N P Pt
Calculated formula	C22 H38 N P Pt
Title of publication	Reactivity Differences of Pt0Phosphine Complexes in C−C Bond Activation of Asymmetric Acetylenes
Authors of publication	Gunay, Ahmet; Müller, Christian; Lachicotte, Rene J.; Brennessel, William W.; Jones, William D.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	22
Pages of publication	6524
a	9.626 ± 0.0006 Å
b	13.2973 ± 0.0008 Å
c	18.3544 ± 0.0011 Å
α	91.231 ± 0.001°
β	94.979 ± 0.001°
γ	94.665 ± 0.001°
Cell volume	2331.8 ± 0.2 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0562
Residual factor for significantly intense reflections	0.0484
Weighted residual factors for significantly intense reflections	0.0724
Weighted residual factors for all reflections included in the refinement	0.0741
Goodness-of-fit parameter for all reflections included in the refinement	1.409
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178586 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/97.	4069795.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069795.cif
40445	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069789, 4069790, 4069791, 4069792, 4069793, 4069794, 4069795, 4069796 via cif-deposit CGI script.	4069795.cif