Crystallography Open Database

Information card for entry 4070465

Preview

Coordinates	4070465.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H46 B Lu N6
Calculated formula	C26 H46 B Lu N6
Title of publication	“Metastable” Lu(GaMe4)3Reacts Like Masked [LuMe3]: Synthesis of an Unsolvated Lanthanide Dimethyl Complex
Authors of publication	Zimmermann, Melanie; Litlabø, Rannveig; Törnroos, Karl W.; Anwander, Reiner
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	23
Pages of publication	6646
a	18.0766 ± 0.0006 Å
b	16.7735 ± 0.0006 Å
c	9.8459 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	2985.35 ± 0.19 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.021
Residual factor for significantly intense reflections	0.0175
Weighted residual factors for significantly intense reflections	0.0433
Weighted residual factors for all reflections included in the refinement	0.0461
Goodness-of-fit parameter for all reflections included in the refinement	1.111
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178593 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/04.	4070465.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4070465.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070465.cif
40729	2012-03-08	../uploads/cif-deposit/cod/cif Adding structures of 4070464, 4070465 via cif-deposit CGI script.	4070465.cif