Crystallography Open Database

Information card for entry 4070603

Preview

Coordinates	4070603.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H32 Ge I N Si
Calculated formula	C17 H32 Ge I N Si
SMILES	C[Ge](C)(C)[Si@](C)(c1ccccc1)C[N+]1(CCCCC1)C.[I-]
Title of publication	Synthesis of a Highly Enantiomerically Enriched Silagermane and Selective Cleavage of the Si−Ge Bond with Lithium
Authors of publication	Strohmann, Carsten; Däschlein, Christian
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	11
Pages of publication	2499
a	17.094 ± 0.006 Å
b	12.559 ± 0.007 Å
c	22.155 ± 0.012 Å
α	90°
β	112.038 ± 0.014°
γ	90°
Cell volume	4409 ± 4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0647
Residual factor for significantly intense reflections	0.0531
Weighted residual factors for significantly intense reflections	0.1274
Weighted residual factors for all reflections included in the refinement	0.1338
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178595 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/06.	4070603.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070603.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070603.cif
42587	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070603 via cif-deposit CGI script.	4070603.cif