Crystallography Open Database

Information card for entry 4070641

Preview

Coordinates	4070641.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H48 N4 Ni2 O6
Calculated formula	C44 H50 N4 Ni2 O6
Title of publication	Binuclear Nickel and Copper Complexes with Bridging 2,5-Diamino-1,4-benzoquinonediimines: Synthesis, Structures, and Catalytic Olefin Polymerization
Authors of publication	Huang, Yuan-Biao; Tang, Guang-Rong; Jin, Gui-Ying; Jin, Guo-Xin
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	2
Pages of publication	259
a	23.63 ± 0.03 Å
b	7.308 ± 0.009 Å
c	16.31 ± 0.02 Å
α	90°
β	128.656 ± 0.017°
γ	90°
Cell volume	2199 ± 5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.2626
Residual factor for significantly intense reflections	0.1341
Weighted residual factors for significantly intense reflections	0.3082
Weighted residual factors for all reflections included in the refinement	0.3778
Goodness-of-fit parameter for all reflections included in the refinement	0.975
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178595 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/06.	4070641.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070641.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070641.cif
42609	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070641 via cif-deposit CGI script.	4070641.cif