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Information card for entry 4070712
Preview
| Coordinates | 4070712.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C74 H89 N3 P Rh Si4 Sn |
|---|---|
| Calculated formula | C74 H89 N3 P Rh Si4 Sn |
| SMILES | [CH]12=[CH]3C4[CH]5=[CH](C1C4)[Rh]235([P](c1ccccc1)(c1ccccc1)c1ccccc1)[Sn]12N(c3cc(cc(c3)C)C)[Si](C)(C)[Si](C)([Si](C)(C)N1c1cc(cc(c1)C)C)[Si](C)(C)N2c1cc(cc(c1)C)C.c1ccccc1.c1ccccc1.c1ccccc1 |
| Title of publication | Triamidostannates(II) as Sterically Demanding Ligands for Rhodium and Iridium |
| Authors of publication | Kilian, Michaela; Wadepohl, Hubert; Gade, Lutz H. |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 4 |
| Pages of publication | 524 |
| a | 12.983 ± 0.0013 Å |
| b | 13.2225 ± 0.0013 Å |
| c | 21.979 ± 0.002 Å |
| α | 95.447 ± 0.002° |
| β | 105.608 ± 0.002° |
| γ | 104.915 ± 0.002° |
| Cell volume | 3456.5 ± 0.6 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0925 |
| Residual factor for significantly intense reflections | 0.0501 |
| Weighted residual factors for significantly intense reflections | 0.112 |
| Weighted residual factors for all reflections included in the refinement | 0.1272 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.99 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178596 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/07. |
4070712.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4070712.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4070712.cif |
| 42655 | 2012-03-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4070709, 4070710, 4070711, 4070712, 4070713, 4070714, 4070715 via cif-deposit CGI script. |
4070712.cif |
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Users of the data should acknowledge the original authors of the
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