Crystallography Open Database

Information card for entry 4070966

Preview

Coordinates	4070966.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H57 Lu N2 Si3
Calculated formula	C30 H57 Lu N2 Si3
Title of publication	Synthesis, Characterization, and Reactivity of the Thermally Stable Lutetium Tris(alkyl) Complex (tBu2bpy)Lu(CH2SiMe3)3
Authors of publication	Masuda, Jason D.; Jantunen, Kimberly C.; Scott, Brian L.; Kiplinger, Jaqueline L.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	6
Pages of publication	1299
a	10.881 ± 0.004 Å
b	29.736 ± 0.011 Å
c	11.509 ± 0.005 Å
α	90°
β	95.423 ± 0.007°
γ	90°
Cell volume	3707 ± 3 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1878
Residual factor for significantly intense reflections	0.0799
Weighted residual factors for significantly intense reflections	0.1057
Weighted residual factors for all reflections included in the refinement	0.1276
Goodness-of-fit parameter for all reflections included in the refinement	0.974
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178598 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/09.	4070966.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070966.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070966.cif
42922	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070966, 4070967, 4070968, 4070969, 4070970 via cif-deposit CGI script.	4070966.cif