Crystallography Open Database

Information card for entry 4071017

Preview

Coordinates	4071017.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H108 O12 Os4 P4 Pd4
Calculated formula	C60 H108 O12 Os4 P4 Pd4
Title of publication	Synthesis and Properties of an Unusual New High-Symmetry Osmium−Palladium Carbonyl Cluster Complex
Authors of publication	Adams, Richard D.; Boswell, Erin M.; Captain, Burjor
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	6
Pages of publication	1169
a	16.4893 ± 0.0002 Å
b	16.4893 ± 0.0002 Å
c	16.4893 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	4483.39 ± 0.09 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	217
Hermann-Mauguin space group symbol	I -4 3 m
Hall space group symbol	I -4 2 3
Residual factor for all reflections	0.0224
Residual factor for significantly intense reflections	0.0221
Weighted residual factors for significantly intense reflections	0.0881
Weighted residual factors for all reflections included in the refinement	0.0883
Goodness-of-fit parameter for all reflections included in the refinement	1.494
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178599 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/10.	4071017.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071017.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071017.cif
42986	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071017 via cif-deposit CGI script.	4071017.cif