Crystallography Open Database

Information card for entry 4071044

Preview

Coordinates	4071044.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C59.5 H53 Cl3 O2.5 Os P3
Calculated formula	C59.5 H53 Cl3 O2.5 Os P3
Title of publication	Synthesis and Characterization of an Air-Stablep-Osmaphenol
Authors of publication	Gong, Lei; Lin, Yumei; He, Guomei; Zhang, Hong; Wang, Huijuan; Wen, Ting Bin; Xia, Haiping
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	3
Pages of publication	309
a	11.438 ± 0.002 Å
b	20.166 ± 0.004 Å
c	14.17 ± 0.003 Å
α	90°
β	113.8°
γ	90°
Cell volume	2990.5 ± 1 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0503
Residual factor for significantly intense reflections	0.0479
Weighted residual factors for significantly intense reflections	0.1222
Weighted residual factors for all reflections included in the refinement	0.1238
Goodness-of-fit parameter for all reflections included in the refinement	1.114
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4071044.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071044.cif
107967	2014-03-25	cif/4 Changing the entity to the proper non-English character for many entries in subdir 4	4071044.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071044.cif
43008	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071044 via cif-deposit CGI script.	4071044.cif