Crystallography Open Database

Information card for entry 4071135

Preview

Coordinates	4071135.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C80 H76 O P4 Pt2 Si2
Calculated formula	C80 H76 O P4 Pt2 Si2
SMILES	[Pt]12([P](c3ccccc3)(c3ccccc3)CC[P]1(c1ccccc1)c1ccccc1)[Si]1([Pt]3([P](c4ccccc4)(c4ccccc4)CC[P]3(c3ccccc3)c3ccccc3)[Si]21(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.O1CCCC1
Title of publication	Ligand Exchange of Diplatinum Complexes with Bridging Silyl Ligands Involving Si−H Bond Cleavage and Formation
Authors of publication	Tanabe, Makoto; Ito, Daisuke; Osakada, Kohtaro
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	10
Pages of publication	2258
a	12.388 ± 0.002 Å
b	13.734 ± 0.002 Å
c	20.297 ± 0.003 Å
α	85.119 ± 0.004°
β	86.097 ± 0.004°
γ	89.294 ± 0.004°
Cell volume	3432.7 ± 0.9 Å³
Cell temperature	113.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.036
Weighted residual factors for all reflections included in the refinement	0.0757
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4071135.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071135.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071135.cif
43062	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071130, 4071131, 4071132, 4071133, 4071134, 4071135 via cif-deposit CGI script.	4071135.cif