Crystallography Open Database

Information card for entry 4071173

Preview

Coordinates	4071173.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H53 I Si4 Sn
Calculated formula	C27 H53 I Si4 Sn
Title of publication	A Stannylene/Aryl Iodide Reagent for Allylic CH Activation and Double Bond Addition Chemistry
Authors of publication	Kavara, Ajdin; Cousineau, Kandarpa D.; Rohr, Ahleah D.; Kampf, Jeff W.; Banaszak Holl, Mark M.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	6
Pages of publication	1041
a	8.8888 ± 0.0008 Å
b	9.563 ± 0.0008 Å
c	20.9269 ± 0.0019 Å
α	91.915 ± 0.001°
β	101.687 ± 0.001°
γ	108.692 ± 0.001°
Cell volume	1640.8 ± 0.3 Å³
Cell temperature	85 ± 2 K
Ambient diffraction temperature	85 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0248
Residual factor for significantly intense reflections	0.0235
Weighted residual factors for significantly intense reflections	0.0541
Weighted residual factors for all reflections included in the refinement	0.0549
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178600 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/11.	4071173.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4071173.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071173.cif
43089	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071173 via cif-deposit CGI script.	4071173.cif