Crystallography Open Database

Information card for entry 4071187

Preview

Coordinates	4071187.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H27 Cl Os
Calculated formula	C18 H27 Cl Os
Title of publication	Synthesis and Protonation Studies of Cp*Os(dppe)H: Kinetic versus Thermodynamic Control
Authors of publication	Dub, Pavel A.; Belkova, Natalia V.; Lyssenko, Konstantin A.; Silantyev, Gleb A.; Epstein, Lina M.; Shubina, Elena S.; Daran, Jean-Claude; Poli, Rinaldo
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	13
Pages of publication	3307
a	14.18 ± 0.003 Å
b	13.87 ± 0.002 Å
c	16.468 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	3238.9 ± 1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0719
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.096
Weighted residual factors for all reflections included in the refinement	0.1173
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178600 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/11.	4071187.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071187.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071187.cif
43098	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071186, 4071187, 4071188 via cif-deposit CGI script.	4071187.cif