Crystallography Open Database

Information card for entry 4071192

Preview

Coordinates	4071192.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H55 N2 Ni O P
Calculated formula	C42 H48 N2 Ni O P
Title of publication	Influence of Steric and Electronic Perturbations on the Polymerization Activities of α-Iminocarboxamide Nickel Complexes
Authors of publication	Azoulay, Jason D.; Itigaki, Koji; Wu, Guang; Bazan, Guillermo C.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	10
Pages of publication	2273
a	9.9429 ± 0.0007 Å
b	25.4501 ± 0.0019 Å
c	15.2227 ± 0.0011 Å
α	90°
β	93.662 ± 0.002°
γ	90°
Cell volume	3844.2 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1315
Residual factor for significantly intense reflections	0.0682
Weighted residual factors for significantly intense reflections	0.1465
Weighted residual factors for all reflections included in the refinement	0.1573
Goodness-of-fit parameter for all reflections included in the refinement	1.451
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178600 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/11.	4071192.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071192.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071192.cif
43099	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071189, 4071190, 4071191, 4071192 via cif-deposit CGI script.	4071192.cif