Crystallography Open Database

Information card for entry 4071203

Preview

Coordinates	4071203.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H25 Cl4 Fe N3
Calculated formula	C24 H25 Cl4 Fe N3
Title of publication	Modification of Iron(II) Tridentate Bis(imino)pyridine Complexes by a Boryl Group for the Production of α-Olefins at High Temperature†
Authors of publication	Ionkin, Alex S.; Marshall, William J.; Adelman, Douglas J.; Fones, Barbara Bobik; Fish, Brian M.; Schiffhauer, Matthew F.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	8
Pages of publication	1902
a	10.414 ± 0.0005 Å
b	15.2465 ± 0.0008 Å
c	15.8488 ± 0.0008 Å
α	90°
β	92.365 ± 0.001°
γ	90°
Cell volume	2514.3 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0602
Residual factor for significantly intense reflections	0.0365
Weighted residual factors for significantly intense reflections	0.0749
Weighted residual factors for all reflections included in the refinement	0.0836
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178601 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/12.	4071203.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071203.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071203.cif
43103	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071203, 4071204, 4071205, 4071206, 4071207, 4071208 via cif-deposit CGI script.	4071203.cif