Crystallography Open Database

Information card for entry 4071295

Preview

Coordinates	4071295.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C70 H109 N8 Ni Sn4
Calculated formula	C70 H109 N8 Ni Sn4
Title of publication	Homoleptic Complexes of Bisstannylenes with Nickel(0): Synthesis, X-Ray Diffraction Studies, and119Sn NMR Investigations
Authors of publication	Zabula, Alexander V.; Pape, Tania; Hepp, Alexander; Hahn, F. Ekkehardt
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	12
Pages of publication	2756
a	18.149 ± 0.005 Å
b	12.499 ± 0.004 Å
c	32.399 ± 0.01 Å
α	90°
β	101.773 ± 0.007°
γ	90°
Cell volume	7195 ± 4 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1467
Residual factor for significantly intense reflections	0.0707
Weighted residual factors for significantly intense reflections	0.1044
Weighted residual factors for all reflections included in the refinement	0.1259
Goodness-of-fit parameter for all reflections included in the refinement	0.976
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178601 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/12.	4071295.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071295.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071295.cif
43140	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071295 via cif-deposit CGI script.	4071295.cif