Crystallography Open Database

Information card for entry 4071299

Preview

Coordinates	4071299.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H34 Cl2 N O3 V
Calculated formula	C25 H34 Cl2 N O3 V
SMILES	[V]1(Cl)(Cl)(Oc2c(cccc2C=[N]1c1ccccc1)C(C)(C)C)([O]1CCCC1)[O]1CCCC1
Title of publication	Synthesis, Structural Characterization, and Ethylene Polymerization Behavior of the Vanadium(III) Complexes Bearing Salicylaldiminato Ligands
Authors of publication	Wu, Ji-Qian; Pan, Li; Hu, Ning-Hai; Li, Yue-Sheng
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	15
Pages of publication	3840
a	7.5894 ± 0.0008 Å
b	13.7589 ± 0.0014 Å
c	24.542 ± 0.003 Å
α	90°
β	96.35 ± 0.002°
γ	90°
Cell volume	2547 ± 0.5 Å³
Cell temperature	187 ± 2 K
Ambient diffraction temperature	187 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1686
Residual factor for significantly intense reflections	0.0704
Weighted residual factors for significantly intense reflections	0.0859
Weighted residual factors for all reflections included in the refinement	0.1016
Goodness-of-fit parameter for all reflections included in the refinement	0.921
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178601 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/12.	4071299.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071299.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071299.cif
43142	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071297, 4071298, 4071299, 4071300, 4071301, 4071302, 4071303, 4071304, 4071305, 4071306 via cif-deposit CGI script.	4071299.cif