Crystallography Open Database

Information card for entry 4071317

Preview

Coordinates	4071317.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H82 Li2 N4 O4 P2 Si2
Calculated formula	C40 H82 Li2 N4 O4 P2 Si2
SMILES	[Si]1(C)(C)(C)N2P(=Cc3c4C=P(C(C)C)(C(C)C)N([Si](C)(C)C)[Li]([n]4cc[n]3[Li]12([O]1CCCC1)[O]1CCCC1)([O]1CCCC1)[O]1CCCC1)(C(C)C)C(C)C
Title of publication	Synthesis of Heteroleptic Tin(II) and Lead(II) Compounds from Pyrazyl-Linked Bisphosphoranoimine
Authors of publication	Leung, Wing-Por; Chan, Ka-Po; Kan, Kwok-Wai; Mak, Thomas C. W.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	12
Pages of publication	2767
a	10.186 ± 0.002 Å
b	15.616 ± 0.003 Å
c	18.308 ± 0.004 Å
α	105.08 ± 0.03°
β	99.53 ± 0.03°
γ	108.25 ± 0.03°
Cell volume	2571.7 ± 1.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1806
Residual factor for significantly intense reflections	0.0699
Weighted residual factors for significantly intense reflections	0.178
Weighted residual factors for all reflections included in the refinement	0.2272
Goodness-of-fit parameter for all reflections included in the refinement	0.994
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178602 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/13.	4071317.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071317.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071317.cif
43146	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071317 via cif-deposit CGI script.	4071317.cif