Crystallography Open Database

Information card for entry 4071326

Preview

Coordinates	4071326.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H25 Cl F3 N2 Rh
Calculated formula	C24 H25 Cl F3 N2 Rh
Title of publication	Rhodium and Iridium Complexes of Abnormal N-Heterocyclic Carbenes Derived from Imidazo[1,2-a]pyridine
Authors of publication	Song, Guoyong; Zhang, Yao; Li, Xingwei
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	8
Pages of publication	1936
a	11.7872 ± 0.0004 Å
b	16.2148 ± 0.0006 Å
c	11.9178 ± 0.0004 Å
α	90°
β	102.218 ± 0.002°
γ	90°
Cell volume	2226.22 ± 0.14 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0645
Residual factor for significantly intense reflections	0.0555
Weighted residual factors for significantly intense reflections	0.1457
Weighted residual factors for all reflections included in the refinement	0.1528
Goodness-of-fit parameter for all reflections included in the refinement	1.194
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178602 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/13.	4071326.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071326.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071326.cif
43155	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071326 via cif-deposit CGI script.	4071326.cif