Crystallography Open Database

Information card for entry 4071330

Preview

Coordinates	4071330.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H36 I3 N8 Rh
Calculated formula	C23 H36 I3 N8 Rh
Title of publication	Rhodium(III) Complexes Containing C4-Bound N-Heterocyclic Carbenes: Synthesis, Coordination Chemistry, and Catalytic Activity in Transfer Hydrogenation
Authors of publication	Yang, Liangru; Krüger, Anneke; Neels, Antonia; Albrecht, Martin
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	13
Pages of publication	3161
a	22.766 ± 0.0009 Å
b	17.1487 ± 0.001 Å
c	18.2406 ± 0.0007 Å
α	90°
β	114.912 ± 0.003°
γ	90°
Cell volume	6458.7 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0448
Residual factor for significantly intense reflections	0.0303
Weighted residual factors for significantly intense reflections	0.07
Weighted residual factors for all reflections included in the refinement	0.0732
Goodness-of-fit parameter for all reflections included in the refinement	0.945
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178602 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/13.	4071330.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071330.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071330.cif
43156	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071327, 4071328, 4071329, 4071330, 4071331, 4071332, 4071333, 4071334 via cif-deposit CGI script.	4071330.cif