Crystallography Open Database

Information card for entry 4071363

Preview

Coordinates	4071363.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H60 O17 P3 Re Sn
Calculated formula	C32 H60 O17 P3 Re Sn
Title of publication	Preparation of Trivinylstannyl Complexes of Manganese and Rhenium
Authors of publication	Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; Fontán, Soledad García; Zanardo, Gianluigi
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	12
Pages of publication	2789
a	10.7012 ± 0.0013 Å
b	22.898 ± 0.003 Å
c	20.818 ± 0.003 Å
α	90°
β	93.557 ± 0.003°
γ	90°
Cell volume	5091.3 ± 1.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0681
Residual factor for significantly intense reflections	0.0366
Weighted residual factors for significantly intense reflections	0.0834
Weighted residual factors for all reflections included in the refinement	0.0937
Goodness-of-fit parameter for all reflections included in the refinement	0.95
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178602 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/13.	4071363.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071363.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071363.cif
43166	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071363 via cif-deposit CGI script.	4071363.cif