Crystallography Open Database

Information card for entry 4071554

Preview

Coordinates	4071554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H88 N8 Sb4
Calculated formula	C48 H76 N8 Sb4
SMILES	c1(c(CN(C)C)cccc1CN(C)C)[Sb]1[Sb](c2c(cccc2CN(C)C)CN(C)C)[Sb](c2c(cccc2CN(C)C)CN(C)C)[Sb]1c1c(cccc1CN(C)C)CN(C)C
Title of publication	Syntheses and Structures of Ar3Sb5and Ar4Sb4Compounds (Ar = C6H3-2,6-(CH2NMe2)2)
Authors of publication	Dostál, Libor; Jambor, Roman; Růžička, Aleš; Holeček, Jaroslav
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	10
Pages of publication	2169
a	22.928 ± 0.0005 Å
b	22.602 ± 0.0017 Å
c	12.236 ± 0.0008 Å
α	90 ± 0.005°
β	90 ± 0.003°
γ	90 ± 0.004°
Cell volume	6340.9 ± 0.6 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	4
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0584
Residual factor for significantly intense reflections	0.0434
Weighted residual factors for significantly intense reflections	0.1037
Weighted residual factors for all reflections included in the refinement	0.1097
Goodness-of-fit parameter for all reflections included in the refinement	1.114
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178604 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/15.	4071554.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071554.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071554.cif
43914	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071553, 4071554 via cif-deposit CGI script.	4071554.cif