Crystallography Open Database

Information card for entry 4071559

Preview

Coordinates	4071559.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C109 H82 Cl7 N2 O3 Os2 P4 Re
Calculated formula	C109 H82 Cl7 N2 O3 Os2 P4 Re
Title of publication	Heteromultimetallic Transition Metal Complexes Based on Unsymmetrical Platinum(II) Bis-Acetylides
Authors of publication	Packheiser, Rico; Ecorchard, Petra; Rüffer, Tobias; Lang, Heinrich
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	14
Pages of publication	3534
a	9.7379 ± 0.0009 Å
b	20.428 ± 0.002 Å
c	26.946 ± 0.003 Å
α	75.718 ± 0.01°
β	80.444 ± 0.009°
γ	82.966 ± 0.009°
Cell volume	5103.8 ± 0.9 Å³
Cell temperature	100 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0764
Residual factor for significantly intense reflections	0.0559
Weighted residual factors for significantly intense reflections	0.1573
Weighted residual factors for all reflections included in the refinement	0.1709
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178604 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/15.	4071559.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071559.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071559.cif
43919	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071559 via cif-deposit CGI script.	4071559.cif