Crystallography Open Database

Information card for entry 4071613

Preview

Coordinates	4071613.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H41 F3 Ge N2 O3 S
Calculated formula	C30 H41 F3 Ge N2 O3 S
Title of publication	Facile Access to a Stable Divalent Germanium Compound with a Terminal PH2Group and Related PR2Derivatives
Authors of publication	Yao, Shenglai; Brym, Markus; Merz, Klaus; Driess, Matthias
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	14
Pages of publication	3601
a	12.087 ± 0.002 Å
b	13.013 ± 0.003 Å
c	24.046 ± 0.005 Å
α	90°
β	92.11 ± 0.03°
γ	90°
Cell volume	3779.6 ± 1.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1054
Residual factor for significantly intense reflections	0.0591
Weighted residual factors for significantly intense reflections	0.1381
Weighted residual factors for all reflections included in the refinement	0.1561
Goodness-of-fit parameter for all reflections included in the refinement	0.93
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178605 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/16.	4071613.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071613.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071613.cif
43946	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071609, 4071610, 4071611, 4071612, 4071613 via cif-deposit CGI script.	4071613.cif