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Information card for entry 4071683
Preview
| Coordinates | 4071683.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C19 H19 N2 Rh |
|---|---|
| Calculated formula | C19 H19 N2 Rh |
| SMILES | [Rh]1234([n]5cccc6cc7cccn1c7c56)[CH]1=[CH]2CC[CH]3=[CH]4CC1 |
| Title of publication | Syntheses, Characterizations, and Reactivities of 4,5-Diazafluorenide Complexes of Palladium(II) and Rhodium(I) |
| Authors of publication | Jiang, Huiling; Song, Datong |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 14 |
| Pages of publication | 3587 |
| a | 10.0544 ± 0.0004 Å |
| b | 11.1105 ± 0.0005 Å |
| c | 12.8356 ± 0.0003 Å |
| α | 90° |
| β | 97.249 ± 0.002° |
| γ | 90° |
| Cell volume | 1422.4 ± 0.09 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0345 |
| Residual factor for significantly intense reflections | 0.0272 |
| Weighted residual factors for significantly intense reflections | 0.0646 |
| Weighted residual factors for all reflections included in the refinement | 0.0686 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301830 (current) | 2025-08-20 | Add cross-references to PubChem compounds in COD range 4/07/ Each referenced PubChem compound corresponds to the full crystal structure. |
4071683.cif |
| 178605 | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/16. |
4071683.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4071683.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4071683.cif |
| 43978 | 2012-03-15 | ../uploads/cif-deposit/cod/cif Adding structures of 4071681, 4071682, 4071683 via cif-deposit CGI script. |
4071683.cif |
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Users of the data should acknowledge the original authors of the
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