Crystallography Open Database

Information card for entry 4071841

Preview

Coordinates	4071841.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Uran-lithium
Formula	C42 H65 Cl3 Li O2 Si2 U2
Calculated formula	C42 H65 Cl3 Li O2 Si2 U2
Title of publication	Coordinative Unsaturation versus Oxophilicity:ansaDimethylsilyl Oxo-Bridged Uranium Metallocenes. Synthesis, Structures, and Unexpected Catalytic Activity with Alkynes and Silanes
Authors of publication	Wang, Jiaxi; Gurevich, Ylia; Botoshansky, Mark; Eisen, Moris S.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	17
Pages of publication	4494
a	15.052 ± 0.003 Å
b	10.636 ± 0.002 Å
c	28.982 ± 0.006 Å
α	90°
β	97.33 ± 0.03°
γ	90°
Cell volume	4601.9 ± 1.6 Å³
Cell temperature	230 ± 1 K
Ambient diffraction temperature	230 ± 1 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1677
Residual factor for significantly intense reflections	0.065
Weighted residual factors for significantly intense reflections	0.1167
Weighted residual factors for all reflections included in the refinement	0.1513
Goodness-of-fit parameter for all reflections included in the refinement	0.944
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178607 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/18.	4071841.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4071841.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071841.cif
44073	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071841 via cif-deposit CGI script.	4071841.cif