Crystallography Open Database

Information card for entry 4071884

Preview

Coordinates	4071884.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H32 Fe2 N3 O2.5
Calculated formula	C24 H32 Fe2 N3 O2.5
Title of publication	Addition of Isocyanides at Diiron μ-Vinyliminium Complexes: Synthesis of Novel Ketenimine−Bis(alkylidene) Complexes
Authors of publication	Busetto, Luigi; Marchetti, Fabio; Zacchini, Stefano; Zanotti, Valerio
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	19
Pages of publication	5058
a	30.013 ± 0.003 Å
b	14.6744 ± 0.0017 Å
c	11.5698 ± 0.0013 Å
α	90°
β	99.67 ± 0.002°
γ	90°
Cell volume	5023.2 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0504
Residual factor for significantly intense reflections	0.0362
Weighted residual factors for significantly intense reflections	0.1076
Weighted residual factors for all reflections included in the refinement	0.1154
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4071884.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4071884.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071884.cif
44096	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071884 via cif-deposit CGI script.	4071884.cif