Crystallography Open Database

Information card for entry 4071900

4071899 << 4071900 >> 4071901

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Coordinates	4071900.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H36 Cl6 N O2 Os P
Calculated formula	C34 H32 Cl6 N O2 Os P
Title of publication	Osmium-Catalyzed Allylic Alkylation
Authors of publication	Esteruelas, Miguel A.; García-Yebra, Cristina; Oliván, Montserrat; Oñate, Enrique; Valencia, Marta
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	19
Pages of publication	4892
a	11.3914 ± 0.0017 Å
b	12.7982 ± 0.0019 Å
c	13.092 ± 0.0019 Å
α	90.109 ± 0.003°
β	107.61 ± 0.002°
γ	103.228 ± 0.003°
Cell volume	1765.7 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	1
Hermann-Mauguin space group symbol	P 1
Hall space group symbol	P 1
Residual factor for all reflections	0.0533
Residual factor for significantly intense reflections	0.0459
Weighted residual factors for significantly intense reflections	0.1091
Weighted residual factors for all reflections included in the refinement	0.1131
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178608 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/19.	4071900.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4071900.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071900.cif
44104	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071900, 4071901, 4071902, 4071903 via cif-deposit CGI script.	4071900.cif