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Information card for entry 4071908
Preview
| Coordinates | 4071908.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H48 N O U |
|---|---|
| Calculated formula | C36 H48 N O U |
| SMILES | [U]12345678([O]9CCCC9)(N(c9ccccc9)c9ccccc9)([c]9([c]1([c]2([c]3([c]49C)C)C)C)C)[c]1([c]5([c]6([c]7([c]81C)C)C)C)C |
| Title of publication | Tetravalent and Pentavalent Uranium Acetylide Complexes Prepared by Oxidative Functionalization with CuCCPh |
| Authors of publication | Graves, Christopher R.; Scott, Brian L.; Morris, David E.; Kiplinger, Jaqueline L. |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 14 |
| Pages of publication | 3335 |
| a | 10.635 ± 0.002 Å |
| b | 10.736 ± 0.002 Å |
| c | 15.299 ± 0.003 Å |
| α | 82.214 ± 0.002° |
| β | 88.185 ± 0.002° |
| γ | 64.197 ± 0.002° |
| Cell volume | 1557.4 ± 0.5 Å3 |
| Cell temperature | 120 ± 1 K |
| Ambient diffraction temperature | 120 ± 1 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0558 |
| Residual factor for significantly intense reflections | 0.0392 |
| Weighted residual factors for significantly intense reflections | 0.0716 |
| Weighted residual factors for all reflections included in the refinement | 0.077 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.98 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178608 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/19. |
4071908.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4071908.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4071908.cif |
| 44109 | 2012-03-15 | ../uploads/cif-deposit/cod/cif Adding structures of 4071908, 4071909 via cif-deposit CGI script. |
4071908.cif |
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Users of the data should acknowledge the original authors of the
structural data.