Crystallography Open Database

Information card for entry 4071912

4071911 << 4071912 >> 4071913

Preview

Coordinates	4071912.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H29 O7 Os3 P
Calculated formula	C27 H29 O7 Os3 P
Title of publication	Activation of Hydrogen and Related Small Molecules by the Unsaturated Cluster Complex PtOs3(CO)7(PBut3)(μ-PBut2)(μ4-CHCMeCH)
Authors of publication	Adams, Richard D.; Boswell, Erin M.; Hall, Michael B.; Yang, Xinzheng
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	19
Pages of publication	4938
a	9.0338 ± 0.0008 Å
b	10.632 ± 0.0009 Å
c	15.8388 ± 0.0014 Å
α	79.472 ± 0.002°
β	82.389 ± 0.002°
γ	84.241 ± 0.002°
Cell volume	1478 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0532
Residual factor for significantly intense reflections	0.0403
Weighted residual factors for significantly intense reflections	0.1005
Weighted residual factors for all reflections included in the refinement	0.1079
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178608 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/19.	4071912.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4071912.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071912.cif
44112	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071912 via cif-deposit CGI script.	4071912.cif