Crystallography Open Database

Information card for entry 4072118

Preview

Coordinates	4072118.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H56 B2 P2 Pb Si2
Calculated formula	C22 H56 B2 P2 Pb Si2
Title of publication	Agostic-Type B−H···Pb Interactions Stabilize a Dialkylplumbylene. Structure of and Bonding in [{nPr2P(BH3)}(Me3Si)C(CH2)]2Pb
Authors of publication	Izod, Keith; McFarlane, William; Wills, Corinne; Clegg, William; Harrington, Ross W.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	17
Pages of publication	4386
a	11.4623 ± 0.0008 Å
b	14.0466 ± 0.0012 Å
c	22.4174 ± 0.0015 Å
α	101.861 ± 0.001°
β	93.528 ± 0.001°
γ	114.037 ± 0.001°
Cell volume	3183.1 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0328
Residual factor for significantly intense reflections	0.0246
Weighted residual factors for significantly intense reflections	0.0571
Weighted residual factors for all reflections included in the refinement	0.0607
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178610 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/21.	4072118.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4072118.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072118.cif
44246	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4072117, 4072118 via cif-deposit CGI script.	4072118.cif