Crystallography Open Database

Information card for entry 4072148

Preview

Coordinates	4072148.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H63 Cl4 N4 O2 P Ru
Calculated formula	C41 H63 Cl4 N4 O2 P Ru
Title of publication	Neutral Ruthenium Carbene Complexes bearing N,N,O Heteroscorpionate Ligands: Syntheses and Activity in Metathesis Reactions
Authors of publication	Kopf, Henning; Holzberger, Bastian; Pietraszuk, Cezary; Hübner, Eike; Burzlaff, Nicolai
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	22
Pages of publication	5894
a	32.805 ± 0.01 Å
b	14.103 ± 0.007 Å
c	20.868 ± 0.009 Å
α	90°
β	110.59 ± 0.03°
γ	90°
Cell volume	9038 ± 7 Å³
Cell temperature	188 ± 2 K
Ambient diffraction temperature	188 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0749
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.1012
Weighted residual factors for all reflections included in the refinement	0.1133
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178610 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/21.	4072148.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4072148.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072148.cif
44263	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4072146, 4072147, 4072148, 4072149 via cif-deposit CGI script.	4072148.cif