Crystallography Open Database

Information card for entry 4072152

Preview

Coordinates	4072152.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22.5 H51.5 I N Si2 U
Calculated formula	C27.5 H51.5 I N Si2 U
Title of publication	A Mild Protocol To Generate Uranium(IV) Mixed-Ligand Metallocene Complexes using Copper(I) Iodide
Authors of publication	Graves, Christopher R.; Schelter, Eric J.; Cantat, Thibault; Scott, Brian L.; Kiplinger, Jaqueline L.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	20
Pages of publication	5371
a	9.76 ± 0.002 Å
b	17.856 ± 0.004 Å
c	18.371 ± 0.004 Å
α	95.73 ± 0.03°
β	100.47 ± 0.03°
γ	93.31 ± 0.03°
Cell volume	3123.1 ± 1.2 Å³
Cell temperature	141 ± 2 K
Ambient diffraction temperature	141 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.041
Residual factor for significantly intense reflections	0.0264
Weighted residual factors for significantly intense reflections	0.0469
Weighted residual factors for all reflections included in the refinement	0.0496
Goodness-of-fit parameter for all reflections included in the refinement	0.983
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4072152.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4072152.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072152.cif
44265	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4072151, 4072152, 4072153, 4072154, 4072155 via cif-deposit CGI script.	4072152.cif