Crystallography Open Database

Information card for entry 4072222

Preview

Coordinates	4072222.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H74 B Br2 Cl6 P2 Pt
Calculated formula	C42 H74 B Br2 Cl6 P2 Pt
Title of publication	Syntheses and Structures of Mono- and Dinuclear Cationic Base-Stabilized Platinum Borylene Complexes
Authors of publication	Braunschweig, Holger; Radacki, Krzysztof; Uttinger, Katharina
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	22
Pages of publication	6005
a	12.7827 ± 0.0004 Å
b	24.4857 ± 0.0007 Å
c	16.2173 ± 0.0005 Å
α	90°
β	90.412 ± 0.002°
γ	90°
Cell volume	5075.8 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0493
Residual factor for significantly intense reflections	0.0314
Weighted residual factors for significantly intense reflections	0.0638
Weighted residual factors for all reflections included in the refinement	0.0711
Goodness-of-fit parameter for all reflections included in the refinement	1.11
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178611 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/22.	4072222.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4072222.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072222.cif
44300	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4072219, 4072220, 4072221, 4072222, 4072223, 4072224 via cif-deposit CGI script.	4072222.cif