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Information card for entry 4072267
Preview
| Coordinates | 4072267.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H46 Ge2 N4 |
|---|---|
| Calculated formula | C30 H46 Ge2 N4 |
| SMILES | [Ge]1([Ge]2[N](=C(N2C(C)(C)C)c2ccccc2)C(C)(C)C)[N](=C(N1C(C)(C)C)c1ccccc1)C(C)(C)C |
| Title of publication | RGe(I)Ge(I)R Compound (R = PhC(NtBu)2) with a Ge−Ge Single Bond and a Comparison with the Gauche Conformation of Hydrazine† |
| Authors of publication | Nagendran, Selvarajan; Sen, Sakya S.; Roesky, Herbert W.; Koley, Debasis; Grubmüller, Helmut; Pal, Aritra; Herbst-Irmer, Regine |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 21 |
| Pages of publication | 5459 |
| a | 20.397 ± 0.003 Å |
| b | 14.12 ± 0.002 Å |
| c | 21.943 ± 0.003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 6319.7 ± 1.6 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.0467 |
| Residual factor for significantly intense reflections | 0.0299 |
| Weighted residual factors for significantly intense reflections | 0.0661 |
| Weighted residual factors for all reflections included in the refinement | 0.0743 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178611 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/22. |
4072267.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4072267.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4072267.cif |
| 44314 | 2012-03-15 | ../uploads/cif-deposit/cod/cif Adding structures of 4072266, 4072267 via cif-deposit CGI script. |
4072267.cif |
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Users of the data should acknowledge the original authors of the
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