Crystallography Open Database

Information card for entry 4072469

Preview

Coordinates	4072469.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H78 F6 N P5 Ru2
Calculated formula	C47 H78 F6 N P5 Ru2
Title of publication	Preparation of Dinuclear Vinylidene Complexes and Their New Deprotonation Reactions
Authors of publication	Liu, Chung-Wei; Lin, Ying-Chih; Huang, Shou-Ling; Cheng,; Liu, Yi-Hung; Wang, Yu
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	14
Pages of publication	3431
a	9.2924 ± 0.0002 Å
b	21.0916 ± 0.0004 Å
c	27.4615 ± 0.0004 Å
α	90°
β	90.185 ± 0.001°
γ	90°
Cell volume	5382.19 ± 0.17 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.098
Residual factor for significantly intense reflections	0.0612
Weighted residual factors for significantly intense reflections	0.1554
Weighted residual factors for all reflections included in the refinement	0.1774
Goodness-of-fit parameter for all reflections included in the refinement	1.089
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178613 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/24.	4072469.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4072469.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072469.cif
45836	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4072469 via cif-deposit CGI script.	4072469.cif