Crystallography Open Database

Information card for entry 4072664

Preview

Coordinates	4072664.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H34 Os2
Calculated formula	C20 H34 Os2
SMILES	[c]12([c]3([c]4([c]5([c]1([Os]16782345[H][Os]23458([H]1)([c]1([c]2([c]3([c]4([c]51C)C)C)C)C)([H]6)[H]7)C)C)C)C)C
Title of publication	Synthesis and Characterization of Osmium Polyhydrides. X-ray Crystal Structures of (C5Me5)OsH5and (C5Me5)2Os2H4
Authors of publication	Gross, Christopher L.; Girolami, Gregory S.
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	1
Pages of publication	160
a	10.098 ± 0.002 Å
b	8.529 ± 0.002 Å
c	12.334 ± 0.002 Å
α	90°
β	108.72 ± 0.03°
γ	90°
Cell volume	1006.1 ± 0.4 Å³
Cell temperature	198 ± 2 K
Ambient diffraction temperature	198 ± 2 K
Number of distinct elements	3
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.0297
Residual factor for significantly intense reflections	0.0246
Weighted residual factors for significantly intense reflections	0.0599
Weighted residual factors for all reflections included in the refinement	0.0631
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178615 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/26.	4072664.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4072664.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072664.cif
45942	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4072664 via cif-deposit CGI script.	4072664.cif