Crystallography Open Database

Information card for entry 4073040

Preview

Coordinates	4073040.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H54 Ru3 Zn
Calculated formula	C32 H49 Ru3 Zn
Title of publication	Ruthenium Polyhydrido Clusters Having a Bridging Alkylzinc Group, [(η5-C5Me5)Ru(μ-H)]3(μ3-ZnR)n(μ3-H)2-nand [(η5-C5Me5)Ru]2(μ-ZnR)n(μ-H)4-n(R = Me and Et;n= 1 and 2)
Authors of publication	Ohashi, Masato; Matsubara, Kouki; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	9
Pages of publication	2330
a	17.237 ± 0.004 Å
b	18.408 ± 0.004 Å
c	11.175 ± 0.003 Å
α	90°
β	104.903 ± 0.014°
γ	90°
Cell volume	3426.5 ± 1.4 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	4
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0455
Residual factor for significantly intense reflections	0.043
Weighted residual factors for significantly intense reflections	0.1188
Weighted residual factors for all reflections included in the refinement	0.1212
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178619 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/30.	4073040.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073040.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073040.cif
46132	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073040, 4073041 via cif-deposit CGI script.	4073040.cif