Crystallography Open Database

Information card for entry 4073185

Preview

Coordinates	4073185.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H20 F2 N2
Calculated formula	C26 H20 F2 N2
SMILES	Fc1ccc(cc1)[CH]N(N(c1ccccc1)[CH]c1ccc(F)cc1)c1ccccc1
Title of publication	Metallic Dysprosium Induced Silyl Radical Reactions: Intermolecular Cyclization and Reduction of Alkynes and Imines
Authors of publication	Zhu, Zhenyu; Wang, Jialiang; Zhang, Zhengxing; Xiang, Xu; Zhou, Xigeng
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	10
Pages of publication	2499
a	8.307 ± 0.006 Å
b	13.991 ± 0.009 Å
c	20.044 ± 0.013 Å
α	110.425 ± 0.007°
β	95.667 ± 0.009°
γ	90 ± 0.009°
Cell volume	2171 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2401
Residual factor for significantly intense reflections	0.134
Weighted residual factors for significantly intense reflections	0.3184
Weighted residual factors for all reflections included in the refinement	0.3932
Goodness-of-fit parameter for all reflections included in the refinement	1.134
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178620 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/31.	4073185.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073185.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073185.cif
46207	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073185 via cif-deposit CGI script.	4073185.cif