Crystallography Open Database

Information card for entry 4073412

Preview

Coordinates	4073412.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H58 I Si6 Tm
Calculated formula	C28 H58 I Si6 Tm
Title of publication	Synthesis and Reactivity of Organometallic Complexes of Divalent Thulium with Cyclopentadienyl and Phospholyl Ligands
Authors of publication	Jaroschik, Florian; Nief, François; Le Goff, Xavier-Frédéric; Ricard, Louis
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	14
Pages of publication	3552
a	40.915 ± 0.002 Å
b	18.358 ± 0.001 Å
c	32.965 ± 0.002 Å
α	90°
β	125.593 ± 0.001°
γ	90°
Cell volume	20134.6 ± 1.9 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0857
Residual factor for significantly intense reflections	0.0433
Weighted residual factors for significantly intense reflections	0.098
Weighted residual factors for all reflections included in the refinement	0.1138
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178623 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/34.	4073412.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073412.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073412.cif
46326	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073411, 4073412, 4073413, 4073414, 4073415, 4073416, 4073417, 4073418 via cif-deposit CGI script.	4073412.cif