Crystallography Open Database

Information card for entry 4073593

Preview

Coordinates	4073593.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	complex 3
Formula	C45 H66 Cu F6 N2 P3
Calculated formula	C45 H66 Cu F6 N2 P3
Title of publication	Synthesis, Structures, and Catalytic Properties of Late-Transition-Metal 2,6-Bis(2-phosphaethenyl)pyridine Complexes
Authors of publication	Hayashi, Akito; Okazaki, Masaaki; Ozawa, Fumiyuki; Tanaka, Rika
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	21
Pages of publication	5246
a	11.73 ± 0.003 Å
b	13.31 ± 0.003 Å
c	18.69 ± 0.005 Å
α	95.4 ± 0.005°
β	95.81 ± 0.004°
γ	110.56 ± 0.005°
Cell volume	2691.6 ± 1.2 Å³
Cell temperature	223.2 K
Ambient diffraction temperature	223 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0866
Weighted residual factors for all reflections included in the refinement	0.1865
Goodness-of-fit parameter for all reflections included in the refinement	1.742
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178624 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/35.	4073593.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073593.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073593.cif
46439	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073593 via cif-deposit CGI script.	4073593.cif