Crystallography Open Database

Information card for entry 4073866

Preview

Coordinates	4073866.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H114 F18 Ir6 N12 O30 S6
Calculated formula	C103 H114 F3 Ir6 N12 O15 S
Title of publication	Stepwise Formation of Tetra- and Hexanuclear Iridium and Rhodium Complexes Containing Oxalato Ligands
Authors of publication	Han, Ying-Feng; Lin, Yue-Jian; Jia, Wei-Guo; Weng, Lin-Hong; Jin, Guo-Xin
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	24
Pages of publication	5848
a	50.627 ± 0.01 Å
b	50.627 ± 0.01 Å
c	50.627 ± 0.01 Å
α	90°
β	90°
γ	90°
Cell volume	129762 ± 4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	228
Hermann-Mauguin space group symbol	F d -3 c :2
Hall space group symbol	-F 4ud 2vw 3
Residual factor for all reflections	0.101
Residual factor for significantly intense reflections	0.0604
Weighted residual factors for significantly intense reflections	0.1376
Weighted residual factors for all reflections included in the refinement	0.1516
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178627 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/38.	4073866.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073866.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073866.cif
46594	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073866 via cif-deposit CGI script.	4073866.cif