Crystallography Open Database

Information card for entry 4073941

Preview

Coordinates	4073941.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H72 Si12
Calculated formula	C24 H72 Si12
Title of publication	Rearrangement of Cyclic Silanes with Aluminum Trichloride
Authors of publication	Wagner, Harald; Wallner, Andreas; Fischer, Jelena; Flock, Michaela; Baumgartner, Judith; Marschner, Christoph
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	27
Pages of publication	6704
a	19.235 ± 0.004 Å
b	12.713 ± 0.003 Å
c	10.285 ± 0.002 Å
α	90°
β	118.53 ± 0.03°
γ	90°
Cell volume	2209.6 ± 1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	3
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0638
Residual factor for significantly intense reflections	0.0573
Weighted residual factors for significantly intense reflections	0.1552
Weighted residual factors for all reflections included in the refinement	0.1592
Goodness-of-fit parameter for all reflections included in the refinement	1.115
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178628 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/39.	4073941.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073941.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073941.cif
46640	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073939, 4073940, 4073941, 4073942, 4073943, 4073944, 4073945, 4073946, 4073947, 4073948 via cif-deposit CGI script.	4073941.cif