Crystallography Open Database

Information card for entry 4074532

Preview

Coordinates	4074532.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C145 H127 Ag8 Cl3 Cu6 Fe12 O9
Calculated formula	C145 H110 Ag8 Cl3 Cu6 Fe12 O9
Title of publication	Rhombic Dodecahedral Ag8M6(M = Cu, Ag, Au) Cluster Complexes of Ferrocenylethynyl Prepared by Reaction of (AgC⋮CFc)nwith [M2(Ph2PNHPh2)2(MeCN)2]2+(M = Cu, Ag, Au)
Authors of publication	Wei, Qiao-Hua; Yin, Gang-Qiang; Zhang, Li-Yi; Chen, Zhong-Ning
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	21
Pages of publication	4941
a	16.261 ± 0.005 Å
b	18.153 ± 0.007 Å
c	27.627 ± 0.009 Å
α	87.95 ± 0.011°
β	75.424 ± 0.01°
γ	74.763 ± 0.007°
Cell volume	7611 ± 5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1388
Residual factor for significantly intense reflections	0.0867
Weighted residual factors for significantly intense reflections	0.2629
Weighted residual factors for all reflections included in the refinement	0.3029
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178634 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/45.	4074532.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074532.cif
48437	2012-03-26	../uploads/cif-deposit/cod/cif Adding structures of 4074531, 4074532, 4074533, 4074534 via cif-deposit CGI script.	4074532.cif