Crystallography Open Database

Information card for entry 4074549

Preview

Coordinates	4074549.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H28 Al3 F12 N2 P Se
Calculated formula	C24 H28 Al3 F12 N2 P Se
Title of publication	Ligand Design for the Assembly of Polynuclear Complexes: Syntheses and Structures of Trinuclear and Tetranuclear Aluminum Alkyl Complexes Bearing Tripodal Diamidoselenophosphinito Ligands and a Comparison to Related Tripodal Triamidophosphine Complexes
Authors of publication	Han, Hua; Johnson, Samuel A.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	23
Pages of publication	5594
a	9.0018 ± 0.0016 Å
b	13.892 ± 0.003 Å
c	13.947 ± 0.003 Å
α	68.85 ± 0.002°
β	85.035 ± 0.002°
γ	88.038 ± 0.002°
Cell volume	1620.5 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.0366
Weighted residual factors for significantly intense reflections	0.0982
Weighted residual factors for all reflections included in the refinement	0.1013
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178634 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/45.	4074549.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074549.cif
48443	2012-03-26	../uploads/cif-deposit/cod/cif Adding structures of 4074546, 4074547, 4074548, 4074549, 4074550, 4074551, 4074552, 4074553 via cif-deposit CGI script.	4074549.cif