Crystallography Open Database

Information card for entry 4074552

Preview

Coordinates	4074552.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H27 Al2 F18 N3 P
Calculated formula	C33 H27 Al2 F18 N3 P
Title of publication	Ligand Design for the Assembly of Polynuclear Complexes: Syntheses and Structures of Trinuclear and Tetranuclear Aluminum Alkyl Complexes Bearing Tripodal Diamidoselenophosphinito Ligands and a Comparison to Related Tripodal Triamidophosphine Complexes
Authors of publication	Han, Hua; Johnson, Samuel A.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	23
Pages of publication	5594
a	11.2709 ± 0.0015 Å
b	11.6947 ± 0.0015 Å
c	15.652 ± 0.002 Å
α	68.451 ± 0.001°
β	86.064 ± 0.001°
γ	78.921 ± 0.001°
Cell volume	1883.1 ± 0.4 Å³
Cell temperature	446 ± 2 K
Ambient diffraction temperature	446 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0685
Residual factor for significantly intense reflections	0.0601
Weighted residual factors for significantly intense reflections	0.165
Weighted residual factors for all reflections included in the refinement	0.1747
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178634 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/45.	4074552.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074552.cif
48443	2012-03-26	../uploads/cif-deposit/cod/cif Adding structures of 4074546, 4074547, 4074548, 4074549, 4074550, 4074551, 4074552, 4074553 via cif-deposit CGI script.	4074552.cif