Crystallography Open Database

Information card for entry 4074699

Preview

Coordinates	4074699.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H54 Cl5 Fe4 Ni2 P4
Calculated formula	C65 H54 Cl5 Fe4 Ni2 P4
Title of publication	Stereoselective Synthesis and Coordination Behavior of Phosphorus-Bridged [1.1]Ferrocenophanes
Authors of publication	Imamura, Yuki; Mizuta, Tsutomu; Miyoshi, Katsuhiko
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	4
Pages of publication	882
a	10.076 ± 0.0001 Å
b	16.395 ± 0.0002 Å
c	18.024 ± 0.0003 Å
α	95.883 ± 0.001°
β	100.267 ± 0.001°
γ	92.234 ± 0.001°
Cell volume	2909.4 ± 0.07 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0773
Residual factor for significantly intense reflections	0.054
Weighted residual factors for significantly intense reflections	0.1128
Weighted residual factors for all reflections included in the refinement	0.1223
Goodness-of-fit parameter for all reflections included in the refinement	1.174
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178635 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/46.	4074699.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074699.cif
48677	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4074696, 4074697, 4074698, 4074699, 4074700 via cif-deposit CGI script.	4074699.cif