Crystallography Open Database

Information card for entry 4074721

Preview

Coordinates	4074721.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43.5 H21 Al F15.5 Zr
Calculated formula	C43.5 H21 Al F15.5 Zr
Title of publication	Diversity in Weakly Coordinating Anions. Mono- and Polynuclear Halo(perfluoroaryl)metalates as Cocatalysts for Stereospecific Olefin Polymerization: Synthesis, Structure, and Reactivity
Authors of publication	Chen, Ming-Chou; Roberts, John A. S.; Seyam, Afif M.; Li, Liting; Zuccaccia, Cristiano; Stahl, Nicholas G.; Marks, Tobin J.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	11
Pages of publication	2833
a	11.9646 ± 0.0008 Å
b	21.1165 ± 0.0014 Å
c	30.68 ± 0.002 Å
α	90°
β	101.237 ± 0.001°
γ	90°
Cell volume	7602.7 ± 0.9 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0747
Residual factor for significantly intense reflections	0.0463
Weighted residual factors for significantly intense reflections	0.1161
Weighted residual factors for all reflections included in the refinement	0.136
Goodness-of-fit parameter for all reflections included in the refinement	1.089
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4074721.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074721.cif
48706	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4074714, 4074715, 4074716, 4074717, 4074718, 4074719, 4074720, 4074721, 4074722, 4074723, 4074724 via cif-deposit CGI script.	4074721.cif