Crystallography Open Database

Information card for entry 4074793

Preview

Coordinates	4074793.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69.16 H89.73 Al2 Cl1.34 Cr N2 P4
Calculated formula	C69.16 H85.23 Al2 Cl1.34 Cr N2 P4
Title of publication	Isolation of a Cationic Chromium(II) Species in a Catalytic System for Ethylene Tri- and Tetramerization
Authors of publication	Jabri, Amir; Crewdson, Patrick; Gambarotta, Sandro; Korobkov, Ilia; Duchateau, Robbert
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	3
Pages of publication	715
a	12.366 ± 0.002 Å
b	16.214 ± 0.003 Å
c	21.347 ± 0.004 Å
α	96.191 ± 0.003°
β	106.453 ± 0.003°
γ	91.839 ± 0.003°
Cell volume	4072.1 ± 1.3 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1041
Residual factor for significantly intense reflections	0.0781
Weighted residual factors for significantly intense reflections	0.2015
Weighted residual factors for all reflections included in the refinement	0.2229
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178636 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/47.	4074793.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074793.cif
48825	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4074793 via cif-deposit CGI script.	4074793.cif