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Information card for entry 4074806
Preview
| Coordinates | 4074806.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H26 N3 O2 P Rh2 Si |
|---|---|
| Calculated formula | C28 H26 N3 O2 P Rh2 Si |
| SMILES | [Rh]12([C]([Si](C)(C)C)#C[Rh]3([n]4c(c5[n]3n2c(c5)C[P]1(c1ccccc1)c1ccccc1)cccc4)C#[O])C#[O] |
| Title of publication | Synthesis of a Library of Iridium-Containing Dinuclear Complexes with Bridging PNNN and PNNP Ligands (BL), [LM(μ-BL)M'L']BF4. 2. Preparation, Basic Coordination Properties, and Reactivity of the Carbonyl Complexes |
| Authors of publication | Dubs, Christian; Yamamoto, Toshiki; Inagaki, Akiko; Akita, Munetaka |
| Journal of publication | Organometallics |
| Year of publication | 2006 |
| Journal volume | 25 |
| Journal issue | 6 |
| Pages of publication | 1359 - 1367 |
| a | 13.491 ± 0.008 Å |
| b | 11.856 ± 0.003 Å |
| c | 17.317 ± 0.01 Å |
| α | 90° |
| β | 102.72 ± 0.01° |
| γ | 90° |
| Cell volume | 2702 ± 2 Å3 |
| Cell temperature | 213 K |
| Ambient diffraction temperature | 213 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for significantly intense reflections | 0.0711 |
| Weighted residual factors for all reflections included in the refinement | 0.2125 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.748 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 209811 (current) | 2018-08-16 | cif/4/ Updating bibliography in entries 4060871-4060877, 4074800-4074806. Marking entries 4060871-4060877 as duplicates of entries 4074800-4074806. |
4074806.cif |
| 176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4074806.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4074806.cif |
| 48834 | 2012-03-27 | ../uploads/cif-deposit/cod/cif Adding structures of 4074802, 4074803, 4074804, 4074805, 4074806 via cif-deposit CGI script. |
4074806.cif |
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Users of the data should acknowledge the original authors of the
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