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Information card for entry 4075071
Preview
| Coordinates | 4075071.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C68 H54 B2 F30 O Ta2 |
|---|---|
| Calculated formula | C68 H54 B2 F30 O Ta2 |
| Title of publication | Synthesis of the Cation Complex [TaCp*Me3]+and a Comparison of Its Reactivity with That of [TaCp*Me4]† |
| Authors of publication | Sánchez-Nieves, Javier; Royo, Pascual; Mosquera, Marta E. G. |
| Journal of publication | Organometallics |
| Year of publication | 2006 |
| Journal volume | 25 |
| Journal issue | 9 |
| Pages of publication | 2331 |
| a | 13.5223 ± 0.0012 Å |
| b | 15.006 ± 0.003 Å |
| c | 17.416 ± 0.004 Å |
| α | 81.144 ± 0.018° |
| β | 88.494 ± 0.009° |
| γ | 79.818 ± 0.015° |
| Cell volume | 3436.9 ± 1.1 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0968 |
| Residual factor for significantly intense reflections | 0.0404 |
| Weighted residual factors for significantly intense reflections | 0.0673 |
| Weighted residual factors for all reflections included in the refinement | 0.0782 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.978 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178639 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/50. |
4075071.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4075071.cif |
| 49045 | 2012-03-27 | ../uploads/cif-deposit/cod/cif Adding structures of 4075071 via cif-deposit CGI script. |
4075071.cif |
All data in the COD and the database itself are dedicated to the
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Users of the data should acknowledge the original authors of the
structural data.