Crystallography Open Database

Information card for entry 4075080

Preview

Coordinates	4075080.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H45 F3 Ge O3
Calculated formula	C34 H46.134 F3 Ge O3
Title of publication	Syntheses, Structures, and Reactions of Heptacoordinate Trihalogermanes Bearing a Triarylmethyl-Type Tetradentate Ligand
Authors of publication	Iwanaga, Kohei; Kobayashi, Junji; Kawashima, Takayuki; Takagi, Nozomi; Nagase, Shigeru
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	14
Pages of publication	3388
a	10.093 ± 0.003 Å
b	11.968 ± 0.004 Å
c	14.947 ± 0.005 Å
α	97.379 ± 0.004°
β	98.341 ± 0.004°
γ	105.019 ± 0.004°
Cell volume	1699.1 ± 1 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0357
Residual factor for significantly intense reflections	0.033
Weighted residual factors for significantly intense reflections	0.0819
Weighted residual factors for all reflections included in the refinement	0.0866
Goodness-of-fit parameter for all reflections included in the refinement	1.14
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178639 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/50.	4075080.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075080.cif
49053	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4075079, 4075080, 4075081, 4075082 via cif-deposit CGI script.	4075080.cif